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P423 - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
P423 - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA

P423 – VLS-PGM SIX NSLS-II

Application

Plane grating monochromator (PGM) for soft X-ray synchrotron radiation

Year of delivery

2015

Installation site

SIX beamline at synchrotron radiation source NSLS-II, USA

This monochromator is part of the SIX beamline, dedicated to high resolution soft X-ray scattering experiments. Energy resolution and pointing stability are here of crucial importance.  The long pre-mirror integrated in this monochromator required an adapted design to achieve the requested high stability of mirror and grating pitch rotations. Special attention was payed to block zero-order and stray light by using several water cooled masks and beam stops.

Design Features

  • High-resolution grazing incidence variable line spacing plane grating monochromator (VLS-PGM).

  • Spectral range: 150 – 2000 eV.
  • Optical elements: one plane mirror and three VLS plane gratings.
  • Temperature sensors at internal mechanics, mirror and gratings chin guards, mirror and gratings holders.
  • Active water cooling of all optical elements.

  • Two piezo actuators at the sine-bar rotation mechanisms.

  • Four water cooled, motorized and electrically isolated OFHC baffle blades at the exit flange.
  • Water cooled internal and external zero-order masks.
  • Permanently installed bakeout provisions.
  • Adjustable support structure.

Performance Features

  • High positioning resolution (minimum incremental motion).
  • High pitch rotation stability and repeatability.
  • Minimized mounting induced deformations.

Outer Dimensions

P423 - Outer dimensions - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA

Technical specifications and performance values

General

Vacuum chamber

Chamber type

cylindrical, vertical axis

Main flange

at the top

Material

1.4404 (C < 0.02%)

Base pressure

10-10 mbar range

Optical design parameters

Beam height (entrance)

1400 mm

Beam offset

19.25 mm

Number of plane mirrors

1

Plane mirror dimensions

500 mm x 50 mm x 70 mm

Number of gratings

3

Gratings dimensions

210 mm x 40 mm x 40 mm

Support structure

Adjustment ranges

Vertical translation

± 15 mm

Lateral translation

± 15 mm

Longitudinal translation

± 15 mm

Pitch

± 1°

Roll

± 1°

Yaw

± 1°

Mirror mechanics

Pitch rotation

Range

+1.6° to -12.3°

Resolution (design value)

0.00375 µrad /motor fine step
(1/64, recommended)
0.0047961 µrad /encoder count

Resolution (measured value)

0.50 µrad

Repeatability

0.15 µrad (pitch)

Long-term stability

0.027 µrad

Long-term stability with cooling water (2.2 l /min)

0.028 µrad

Scanning speed

~ 700 µrad /s

Grating mechanics

Pitch rotation

Range

+1.6° to -12.6°

Resolution (design value)

0.00375 µrad /motor fine step
(1/64, recommended)
0.0047961 µrad /encoder count

Resolution (measured value)

0.50 µrad

Repeatability

0.10 µrad (pitch)

Long-term stability

0.011 µrad

Long-term stability with cooling water (1.5 l /min)

0.012 µrad

Scanning speed

~ 700 µrad /s

Translation (grating exchange)

Range

-125 mm to +25.6 mm

Resolution (design value)

0.04 µm /motor fine step
(1/128, recommended)
0.05 µm /encoder count

Repeatability

0.06 µrad (pitch)

0.40 µrad (roll)

Baffle slits

Blades

Material

OFHC

Range

-2 mm to +25 mm

Resolution (design value)

0.10 µm /motor step
(full step at actuator)

Performance Test Results

Pitch deviation after pitch change (mirror)
P423 - Pitch deviation after pitch change (mirror) - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Pitch deviation after pitch change (grating)
P423 - Pitch deviation after pitch change (grating) - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Pitch deviation after grating translation
P423 - Pitch deviation after grating translation - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Roll deviation after grating translation
P423 - Roll deviation after grating translation - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Mirror pitch positioning resolution
P423 - Mirror pitch positioning - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Mirror pitch positioning resolution (2.2 l /min)
P423 - Mirror pitch positioning with water - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Mirror pitch long-term stability
P423 - Mirror pitch stability - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Mirror pitch long-term stability (2.2 l /min)
P423 - Mirror pitch stability with water - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Grating pitch positioning resolution
P423 - Grating pitch positioning - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Grating pitch positioning resolution  (1.5 l /min)
P423 - Grating pitch positioning with water - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Grating pitch long-term stability
P423 - Grating pitch stability - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Grating pitch long-term stability (1.5 l /min)
P423 - Grating pitch stability with water - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Grating pitch stability for different water flow rates
P423 - Grating pitch stability for different flow rates - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Scanning speed of mirror pitch
P423 - Scanning speed of mirror pitch - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Scanning speed of grating pitch
P423 - Scanning speed of grating pitch - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA
Residual gas analysis
P423 - Residual gas analysis - Plane grating monochromator (PGM) for soft X-ray synchrotron radiation at SIX beamline at synchrotron radiation source NSLS-II, USA

Pictures