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P441 - Spherical grating monochromator (SGM) for soft X-ray synchrotron radiation at Beamline I21-IXS at Diamond Light Source, Didcot, United Kingdom
P441 - Spherical grating monochromator (SGM) for soft X-ray synchrotron radiation at Beamline I21-IXS at Diamond Light Source, Didcot, United Kingdom

P441 – SGM I21-IXS DLS

Application

Spherical grating monochromator (SGM) for soft X-ray synchrotron radiation

Year of delivery

2016

Installation site

Beamline I21-IXS at Diamond Light Source, Didcot, United Kingdom

This grating unit was developed and built to be integrated into the high energy resolution RIXS system at I21-IXS at DLS. The challenge was to accomodate all components for standard functionality and for compensation of spectrometer related spurious movements into a very limited space, without perfomance lost.

Design Features

  • Grating unit for high resolution soft X-ray spectrometer.
  • Spectral range: 250 – 3000 eV.
  • Very compact design for integration into the RIXS system.

  • Optical elements: three spherical gratings.
  • Temperature sensors at internal mechanics.
  • Motorized and encoded vertical translation of the internal mechanics for compensation of spurios height and roll variation upon scattering angle change.
  • Permanently installed bakeout provisions.
  • Adjustable support structure.

Performance Features

  • High pitch rotation stability and repeatability.
  • Minimized mounting induced deformations.

Outer Dimensions

P441 - Outer dimensions - Spherical grating monochromator (SGM) for soft X-ray synchrotron radiation at Beamline I21-IXS at Diamond Light Source, Didcot, United Kingdom

Technical specifications and performance values

General

Vacuum chamber

Chamber type

rectangular footprint

Main flanges

at the top

Material

1.4404 (C < 0.02%)

Base pressure

10-10 mbar range

Optical design parameters

Beam height

1415 mm

Number of gratings

3

Grating dimensions

200 mm x 40 mm x 50 mm

Grating mechanics

Pitch rotation

Range

-10.70° to +1.4°

Resolution

0.004 µrad /motor fine step
(1/64, recommended)
0.0047961 µrad /encoder count

Repeatability

0.08 µrad (pitch)

0.20 µrad (roll)

Stability

0.012 µrad

Translation (grating exchange)

Range

-115.3 mm to +76.3 mm

Resolution (design value)

0.40 µm /motor fine step
(1/128, recommended)
0.05 µm /encoder count

Repeatability

0.20 µrad (pitch)

0.17 µrad (roll)

Translation (grating height)

Range

-1.18 mm to +1.13 mm
(wedge leveler 1)
-1.15 mm to +1.48 mm
(wedge leveler 2)

Resolution (design value)

0.40 µm /motor step (at actuator)
0.02 µm /motor step
(at wedge leveler)
0.005 µm /encoder count

Performance Test Results

Pitch deviation after pitch change
P441 - Pitch deviation after pitch change - Spherical grating monochromator (SGM) for soft X-ray synchrotron radiation at Beamline I21-IXS at Diamond Light Source, Didcot, United Kingdom
Roll deviation after pitch change
P441 - Roll deviation after pitch change - Spherical grating monochromator (SGM) for soft X-ray synchrotron radiation at Beamline I21-IXS at Diamond Light Source, Didcot, United Kingdom
Pitch deviation after grating translation
P441 - Pitch deviation after grating translation - Spherical grating monochromator (SGM) for soft X-ray synchrotron radiation at Beamline I21-IXS at Diamond Light Source, Didcot, United Kingdom
Roll deviation after grating translation
P441 - Roll deviation after grating translation - Spherical grating monochromator (SGM) for soft X-ray synchrotron radiation at Beamline I21-IXS at Diamond Light Source, Didcot, United Kingdom
Grating pitch stability
P441 - Grating pitch stability - Spherical grating monochromator (SGM) for soft X-ray synchrotron radiation at Beamline I21-IXS at Diamond Light Source, Didcot, United Kingdom
Residual gas analysis
P441 - Residual gas analysis - Spherical grating monochromator (SGM) for soft X-ray synchrotron radiation at Beamline I21-IXS at Diamond Light Source, Didcot, United Kingdom

Pictures